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Carbonate Analysis : Carbonate Of Carbon Dioxide Gas

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Tara Winkelmann
CHE 133: 203
Dr. Clementz
28 April 2015
Lab #3: Carbonate Analysis
Purpose
The volume of carbon dioxide gas produced from a reaction was measured in order to determine what carbonate sample was used. A gas assembly apparatus was used to capture the gas from a reaction between an unknown carbonate and 6M hydrochloric acid; three trials were performed. The mass of the unknown carbonate was determined, and the reaction occurred in a test tube. The volume of gas produced by the reaction was measured, and the partial pressure of carbon dioxide was calculated after the partial pressure of water vapor was determined using Dalton’s Law of Partial Pressures. The percent mass of carbon dioxide gas was then calculated, and the average mass percent was compared to the table of known carbonates. It was concluded that the unknown carbonate sample used in the reaction was magnesium carbonate.
Procedure
CHE 133 Experiment 3, General Chemistry II Lab, Spring Quarter 2014-2015, DePaul University. [Online] https://www.d2l.depaul.edu (accessed April 25, 2015) No deviations from the procedure were made.
Data and Results An unknown sample was massed and put into three test tubes for three different trials. A gas transfer assembly was put together and hydrochloric acid was added to each sample in each test tube. A reaction between the carbonate sample and the acid occurred and the volume of carbon dioxide gas produced was recorded. This process was repeated three times. The mass

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