10 Amphetamine: Excellent Response and Peak Symmetry 5 Drug Screen (GC/MS) 10 Column: Equity-5, 30m x 0.25mm ID, 0.25pm Cat. No.: 28089-U 15 Min Oven: 45°C (2 min) to 110°C @ 25°C/min to 200°C @ 15°C/min to 280°C Inj.: 250°C Det.: 5973 MSD, 40-450 amu scan range, 325°C transfer line Flow: Helium, 40psi for 0.2 min then 0.7mL/min constant flow Injection: 0.3μL pulsed splitless @ 50mL/min (0.5 min) Liner: Splitless 2mm ID Sample: -15ng on-column of a 16-component drug standard 2 6 3 1.2,4,5,6-Tetrachloro- m-xylene (surr.) 6. Heptachlor 7. Aldrin 2α-BHC 8. Heptachlor epoxide 3 B-BHC 9. +-Chlordane 4.1-BHC 10. Endosulfan! 5.&-BHC 8 10 11. a-Chlordane 10 1. Amphetamine 2. Methamphetamine 3. Nicotine 4. Caffeine 5. Diphenhydramine 6. Lidocaine 7. Phenobarbital 8. Methadone 9. Amitripyline 10. Cocaine 11. Desipramine 12. Codeine 13. Morphine 14. Diazepam 15. Heroin 16. Fentenyl 13 Key Resolutions Achieved 15 16 GOO1691 12 4,4'-DDE 13. Dieldrin 14. Endrin 15. Endosulfan Il 16 4,4'-DDD 17. Endrin aldehyde 18. Endosulfan sulfate 19. 4,4'-DDT 20. Endrin ketone 21. Methoxychlor 22. Decachlorobiphenyl (sum.) 11 12 13 15 20 16 1819 17 14 20 Min US EPA Method 8081 Chlorinated Pesticides (GC) Column: Equity-5, 30m x 0.25mm ID, 0.25μm Cat. No.: 28089-U Oven: 100°C (2 min) to 160°C @ 15°C/min to 300°C @ S°C/min (10 min) Inj.: 225°C Det.: ECD, 310°C Flow: Helium, 30cm/sec @ 100°C Injection: 2.0pt, splitless (0.5 min) Liner: Splitless double taper, unpacked Sample: 50ppb of a 22 component chlorinated pesticide standard (Cat. No. 46845-U) 21 - 30 22 GOO1689 13
10 Amphetamine: Excellent Response and Peak Symmetry 5 Drug Screen (GC/MS) 10 Column: Equity-5, 30m x 0.25mm ID, 0.25pm Cat. No.: 28089-U 15 Min Oven: 45°C (2 min) to 110°C @ 25°C/min to 200°C @ 15°C/min to 280°C Inj.: 250°C Det.: 5973 MSD, 40-450 amu scan range, 325°C transfer line Flow: Helium, 40psi for 0.2 min then 0.7mL/min constant flow Injection: 0.3μL pulsed splitless @ 50mL/min (0.5 min) Liner: Splitless 2mm ID Sample: -15ng on-column of a 16-component drug standard 2 6 3 1.2,4,5,6-Tetrachloro- m-xylene (surr.) 6. Heptachlor 7. Aldrin 2α-BHC 8. Heptachlor epoxide 3 B-BHC 9. +-Chlordane 4.1-BHC 10. Endosulfan! 5.&-BHC 8 10 11. a-Chlordane 10 1. Amphetamine 2. Methamphetamine 3. Nicotine 4. Caffeine 5. Diphenhydramine 6. Lidocaine 7. Phenobarbital 8. Methadone 9. Amitripyline 10. Cocaine 11. Desipramine 12. Codeine 13. Morphine 14. Diazepam 15. Heroin 16. Fentenyl 13 Key Resolutions Achieved 15 16 GOO1691 12 4,4'-DDE 13. Dieldrin 14. Endrin 15. Endosulfan Il 16 4,4'-DDD 17. Endrin aldehyde 18. Endosulfan sulfate 19. 4,4'-DDT 20. Endrin ketone 21. Methoxychlor 22. Decachlorobiphenyl (sum.) 11 12 13 15 20 16 1819 17 14 20 Min US EPA Method 8081 Chlorinated Pesticides (GC) Column: Equity-5, 30m x 0.25mm ID, 0.25μm Cat. No.: 28089-U Oven: 100°C (2 min) to 160°C @ 15°C/min to 300°C @ S°C/min (10 min) Inj.: 225°C Det.: ECD, 310°C Flow: Helium, 30cm/sec @ 100°C Injection: 2.0pt, splitless (0.5 min) Liner: Splitless double taper, unpacked Sample: 50ppb of a 22 component chlorinated pesticide standard (Cat. No. 46845-U) 21 - 30 22 GOO1689 13
Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter9: Atomic Absorption And Atomic Fluorescence Spectrometry
Section: Chapter Questions
Problem 9.6QAP
Related questions
Question
Does this method in the picture below resolve the components of the drug mixture well of a paper chromatography of metal ions experiment?
Transcribed Image Text:10
Amphetamine:
Excellent Response
and Peak Symmetry
5
Drug Screen (GC/MS)
10
Column: Equity-5, 30m x 0.25mm ID, 0.25pm
Cat. No.:
28089-U
15
Min
Oven: 45°C (2 min) to 110°C @ 25°C/min to 200°C @ 15°C/min to 280°C
Inj.: 250°C
Det.: 5973 MSD, 40-450 amu scan range, 325°C transfer line
Flow: Helium, 40psi for 0.2 min then 0.7mL/min constant flow
Injection: 0.3μL pulsed splitless @ 50mL/min (0.5 min)
Liner:
Splitless 2mm ID
Sample: -15ng on-column of a 16-component drug standard
2
6
3
1.2,4,5,6-Tetrachloro-
m-xylene (surr.)
6. Heptachlor
7. Aldrin
2α-BHC
8. Heptachlor epoxide
3 B-BHC
9. +-Chlordane
4.1-BHC
10. Endosulfan!
5.&-BHC
8
10
11. a-Chlordane
10
1. Amphetamine
2. Methamphetamine
3. Nicotine
4. Caffeine
5. Diphenhydramine
6. Lidocaine
7. Phenobarbital
8. Methadone
9. Amitripyline
10. Cocaine
11. Desipramine
12. Codeine
13. Morphine
14. Diazepam
15. Heroin
16. Fentenyl
13
Key Resolutions
Achieved
15
16
GOO1691
12 4,4'-DDE
13. Dieldrin
14. Endrin
15. Endosulfan Il
16 4,4'-DDD
17. Endrin aldehyde
18. Endosulfan sulfate
19. 4,4'-DDT
20. Endrin ketone
21. Methoxychlor
22. Decachlorobiphenyl (sum.)
11
12
13
15
20
16
1819
17
14
20
Min
US EPA Method 8081 Chlorinated Pesticides (GC)
Column: Equity-5, 30m x 0.25mm ID, 0.25μm
Cat. No.: 28089-U
Oven: 100°C (2 min) to 160°C @ 15°C/min to 300°C @ S°C/min (10 min)
Inj.: 225°C
Det.: ECD, 310°C
Flow:
Helium, 30cm/sec @ 100°C
Injection: 2.0pt, splitless (0.5 min)
Liner: Splitless double taper, unpacked
Sample: 50ppb of a 22 component chlorinated pesticide standard
(Cat. No. 46845-U)
21
-
30
22
GOO1689
13
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