ANSWER 2CNOTE: THIS CAN NOT BE HAND-DRAWN OR WRITTEN. EXPLANATION MUST BE DIGITALLY ILLUSTRATED/TYPED! 2A. What is the theoretical yield and limiting reagent for the Friedel Crafts acylation reaction of tolueneas described in the experiment provided if the reaction is started with 5 g of aluminum chloride, 25 mLof dichloromethane (total), 3.5 g acetyl chloride, and 3.7 mL of toluene?2B. What are the safety precautions used in the experimental procedure provided to prevent exposureto HCI gas?2C. Write the separation scheme for the isolation of 4-methyl acetophenone from the reaction mixturein the experiment provided.

Tthe separation scheme for isolating 4-Methyl Acetophenone from the given reaction mixture as…

Answered: 2C. Write the separation scheme for the…

2C. Write the separation scheme for the isolation of 4-methyl acetophenone from the reaction mixture in the experiment provided.

Organic Chemistry

9th Edition

ISBN:9781305080485

Author:John E. McMurry

Publisher:John E. McMurry

Chapter3: Organic Compounds: Alkanes And Their Stereochemistry

Section3.SE: Something Extra

Problem 50AP: Formaldehyde, H2C=O, is known to all biologists because of its usefulness as a tissue preservative....

See similar textbooks

Related questions

Q: Calculate the ph of a solution prepared by dissolving 1.30 (g) of sodium acetate, CH3COONa, in 92.0…

A: IntroductionSodium acetate, CH3COONa, dissociates into sodium ions (Na+) and acetate ions (CH3COO-)…

Q: A helium-filled weather balloon has a volume of 729 L at 16.9°C and 755 mmHg. It is released and…

A: Initially,P1 = 755 mmHgV1 = 729 LT1 = 16.9°C = (16.9 + 273.15)K = 290.05 KLater,P2 = 454 mmHgV2 =…

Q: f a buffer solution is 0.110 M in a weak acid (K₂ = 6.1 × 10-5) and 0.410 M in its conjugate base,…

A: Suppose weak acid is HA [HA] = 0.110 M[A-] = 0.410 MKa = 6.1 × 10-5

Q: What are the concentrations of H3O+ and OH− in oranges that have a pH of 3.93?

A: pH of the solution = 3.93Concentration of H3O+ = [H3O+] = ?Concentration of OH- = [OH-] = ?

Q: In the space below, enter the letter for the correct answer (not case sensitive). PhOCH2CH2CH3 is…

A: 1. The given molecule has 1 chiral center in the reaction that take place is in aqueous medium which…

Q: The combustion of wood produces an average of 15 000 kJ/kg. Suppose 4.30 kg of wood is burned in a…

A: GivenMass of the wood =The calorific value of wood =.Mass of air = .Specific heat capacity of air,…

Q: 9) Draw the "hexagon" line structure of the following (be sure to indicate stereochemistry). FOLOH…

A: To draw the planar 2D structure of a cyclic ester given in chair form with their respective…

Q: A. 2-methyl-2-pentene (CH3)2C=CHCH2CH3 B. 2-ethyl-1-butene (CH3CH2)2C=CH2 Give the name/s…

A: The reactants are:A. 2-methyl-2-pentene (CH3)2C=CHCH2CH3B. 2-ethyl-1-butene (CH3CH2)2C=CH2The…

Q: Determine the [OH−] , pH, and pOH of a solution with a [H+] of 1.5×10−8 M at 25 °C. Determine the…

A: To solve these problems, we can use the equations relating pH, pOH, [H+], and [OH-] in water For a…

Q: 15. Calculate the maximum amount of work that can be obtained at 25°C from an electrochemical cell…

A: As we know; Standard reduction potential of MnO2 electrodes is +1.230 V whereas for Na-electrode is…

Q: Be sure to answer all parts. What are [H3O+], [OH¯], and pH in a solution with a pOH of 9.34? Make…

A: -> pH and pOH relates as -pH + pOH = 14 -> pH and H3O+ related as - pH = -log[H3O+] ->…

Q: There are 7.83 x 10^10 molecules of (C6H5NO2) Determine the following How many moles are of…

Q: 1B. Write the mechanism for the Friedel Crafts Acylation reaction of ethyl benzene using acetyl…

A: The Friedel-Crafts acylation is a reaction which occurs in the presence of lewis acid AlCl3 The…

Q: Nitric oxide (NO) can be formed from nitrogen, hydrogen and oxygen in two steps. In the first step,…

Q: If a buffer solution is made from 450.0 mL of 3.8 M aniline salt mixed with 400.0 mL of 4.1 M…

Q: vis dot structure of methanol (CH3OH) is given below. Estimate the enthalpy of combustion of ethanol…

A: Enthalpy of the combustion of methanol is to be calculated.

Q: Hydrogen iodide decomposes according to the reaction 2 HI(g) → H₂(g) + I₂(g) A sealed 1.50-L…

Q: 23. Neglecting stereochemistry, which of these common group names is ambiguous, i.e., does not refer…

Q: Give the oxidation number of the underlined atoms in the following molecules or ions: ( ach) 1. CH4…

A: “Since you have posted multiple questions, we will provide the solution only to the first five…

Q: b. CH,MgBr + H₂N,

A: We have to identify the product of the given reagent.

Q: Draw the line structure for (CH3)2CH(CH2)3OC(CH3)3

A: IntroductionIn this structure, the central carbon atom is bonded to two methyl groups (CH3) and one…

Q: The ?a of propanoic acid (C2H5COOH) is 1.34×10−5. Calculate the pH of the solution and the…

Q: 2A. What is the theoretical yield and limiting reagent for the reaction of isopropanol and acetic…

A: IntroductionReversible reactions can be driven towards the formation of products using various…

Q: If a buffer solution is 0.110 M in a weak base (K₁ = 7.2 x 10-5) and 0.460 M in its conjugate acid,…

A: We have concentration of weak base as 0.11 M and concentration of salt as 0.46M .We have to…

Q: A dilute solution is found to contain 6.095 x 10-6 M of cobalt. This solution was prepared when 20.0…

A: M1 = initial molarity = 6.095 × 10-6 MV1 = initial volume = 20.0 mLV2 = final volume = 250.0 mLM2 =…

Q: Draw the major product of each step in this reaction sequence. Ignore inorganic byproducts. O Select…

A: At first presence of Et3N it abstract the alcoholic proton and form alkoxide ion ,then there occurs…

Q: 1) What is the IUPAC name for the compound shown? A) 1-isopropyl-4-cyclopentanol B)…

Q: What is the pH after the addition of 10.0 mL of 0.150 M NaOH to 25.0 mL of 0.115 M HNO3? View…

Q: (y) Which of the drawings above best represents the ions in a solution of Fe(NO3)3(aq)? Example:…

A: In a chemical reaction, when the compound in the aqueous phase breaks down into two or more simpler…

Q: Give the structural formula for compounds A- + CH₂ - CH₂₂ AICI => H₂D A CG₂ H1003) 3 -> 1 COOH COOH…

A: “Since you have posted a question with multiple sub-parts, we will solve first three subparts for…

Q: What is the balanced complete ionic and net ionic equations for this reaction? Thank you

Q: When determining the equilibrium concentrations for the reaction [A][B] [AB] a simplifying…

A: As we know, if your change in concentration value (x in an I.C.E. table) is less than 5% of the…

Q: What is the correct structural formulas for 5-ethylept-4-enal?

A: IntroductionThe main part of the name, "ept-4-enal," suggests that the molecule contains a…

Q: A chemist measures the enthalpy change AH during the following reaction: C6H₁2O6(s)-3 CH₂(g) + 3…

A: -> When reaction is multiplied with constant then enthalpy also multiplied with same…

Q: chemical engineer is studying the two reactions shown in the table below. In each case, she fills a…

A: A spontaneous reaction is a that favors product formation. It is estimated by the negative sign of…

Q: In the laboratory, a general chemistry student measured the pH of a 0.564 M aqueous solution of…

A: Dear student since you have posted multiple questions, As per BARTLEBY QnA guidelines we are allowed…

Q: 8. Which of the following compounds exhibits the strongest London dispersion forces?…

Q: A mixed melting point was determined mixing unknown with benzilic acid (p 144-152), and unknown…

A: Based on the information provided, we can determine the student's unknown compound by analyzing the…

Q: Consider the following structure as you answer the questions below: CH3 CH₂-C-N-CH3 CI Identify the…

Q: (n) H₂N Loe/NaⒸ warm then, dil H₂O work-up

A: Since you have asked multiple question, we will solve the first question for you. If you want any…

Q: Consider the following generic reaction: A + 2B C + 3D, AH-176 kJ. Determine the value of AH for…

A: The thermochemical equations can be treated as algebraic equation which can be added, subtracted,…

Q: t, 5.010 g of acetylene (C₂H₂) a are put into the "bomb" and similarly completely burned in an…

A: The amount of heat released or absorbed during the reaction is to be calculated.Mass of the water =…

Q: What volume of hydrogen gas is produced when 54.0 g of sodium reacts completely according to the…

A: Given,Sodium(s) + water(l) -----> sodium hydroxide(aq) + hydrogen(g)mass of sodium (Na) reacts =…

Q: Which compound will have the larger magnitude enthalpy of hydration? a. LiCl or CsCl? OLICI OCsCl b.…

A: IntroductionThe charges and sizes of the ions involved, and the strength of the ion-dipole…

Q: What volume of hydrogen gas is produced when 93.6 g of iron reacts completely according to the…

A: Since you have asked multiple question, we will solve the first question for you.If you want any…

Q: Metal lithium strontium calcium magnesium zinc copper barium manganese lead arsenic potassium sodium…

A: Flame test is used to identify the group 1 metals.Lithium: The flame color for lithium is…

Q: Place 0.649 mol of a weak acid, HA, and 12.4 g of NaOH in enough water to produce 1.00 L of…

Q: What is reflux?

A: Refluxing is a widely used technique in organic chemistry to maintain a constant temperature…

Q: If you wanted to produce 5.00 grams of iron(III) hydroxide, how many mL of 1.00 M Fe(NO3)3 would you…

A: mass of iron(III) hydroxide (Fe(OH)3) produced = 5.00 gConcentration of Fe(NO3)3 solution= 1.00 M =…

Q: Imagine an alternate universe where the value of the Planck constant is 6.62607 × 10 J.s. In that…

A: The type of mechanics required to describe the given objects is to be selected.

Question

ANSWER 2C

NOTE: THIS CAN NOT BE HAND-DRAWN OR WRITTEN. EXPLANATION MUST BE DIGITALLY ILLUSTRATED/TYPED!

2A. What is the theoretical yield and limiting reagent for the Friedel Crafts acylation reaction of toluene
as described in the experiment provided if the reaction is started with 5 g of aluminum chloride, 25 mL
of dichloromethane (total), 3.5 g acetyl chloride, and 3.7 mL of toluene?
2B. What are the safety precautions used in the experimental procedure provided to prevent exposure
to HCI gas?
2C. Write the separation scheme for the isolation of 4-methyl acetophenone from the reaction mixture
in the experiment provided.

Expert Solution

This question has been solved!

Explore an expertly crafted, step-by-step solution for a thorough understanding of key concepts.

This is a popular solution!

SEE SOLUTION Check out a sample Q&A here

Step 1: Separation scheme

VIEW

Step 2: Steps to follows

VIEW

Solution

VIEW

Trending now

This is a popular solution!

Step by step

Solved in 3 steps

SEE SOLUTION Check out a sample Q&A here

Knowledge Booster

Sample Preparation in Analytical Chemistry

Learn more about

Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.

Similar questions

Several diamines are building blocks for the synthesis of pharmaceuticals and agro-chemicals. Show how both 1,3-propanediamine and 1,4-butanediamine can be prepared from acrylonitrile.
In preparation of p-Nitroaniline, Starting material is 50g of p-nitroacetanilide, 22ml of HCI, 20g of p-nitroaniline. Give % yield of nitro acetanilide.
(a) Tsomane and Nyiko were given a task of synthesising methylenecyclohexane 2. After a brief discussion with each other, Tsomane proposed Method A to synthesise 2 from cyclohexanone 1 while Nyiko proposed Method B that started from hydroxymethylcyclohexane 3. Each student believed that their proposed method is better than the other. (Scheme below) (1) 1 Ph THF A Ph Ph B H₂SO4 100 °C 3 OH What is the name of the reaction that is followed by reaction Method A?
10. M and N are amines with the molecular formula C3H»N. Reaction of M with sodium nitrite and HCI releases nitrogen gas and produces a mixture of X and Y and Propanol while N produces a yellowish oily compound, S when reacted with the same reagents. Give the structures of M, N, X, Y, and S. Outline the synthesis of M from a suitable alkene.
What is the percent yield of the hydroboration oxidation of 1-octene to form 1-octanol? Original amount of 1-octene added 840 uL 2 mL of 1M borane THF added For oxidation 1.2mL of 3M NAOH and 1.2 mL of 30% hydrogen peroxide 2 mL of diethyl ether used for extraction 5.11g obtained as final product.
A student attempted to prepare 1-chlorobutane by mixing 1-butanol with NaCl in acetone. Was the student succesful? Explain.
Benzene is often produced as a side product during Grignard reactions using phenylmagnesium bromide. How can its formation be explained? Give a balanced equation for its formation.
Dimethyl disulfide, CH,S–SCH3, found in the vaginal secretions of female hamsters, acts as a sexual attractant for the male hamster. Write an equation for its synthesis from methanethiol.
8. Under anhydrous conditions, 4.8 mL of 1-bromo-3,5-dimethylbenzene (dens. 1.36 g/mL) is treated with 0.90 g of magnesium in 25 mL of diethyl ether. After the initial reaction, the ether solution is poured over 8.5 grams of dry ice (carbon dioxide). The mixture is then treated with 50 mL 1M aqueous HCl. The resulting biphasic mixture is transferred to a separatory funnel and the aqueous layer is removed. The organic layer that remains in the separatory funnel is then treated with 20 mL 3M aqueous NaOH. After shaking the separatory funnel and allowing the layers to separate, the aqueous layer is removed and treated with aqueous 6M HCl until a precipitate forms and the pH of the solution acidic by pH paper. The precipitate is isolated by vacuum filtration and allowed to dry resulting in 3.73 g of a white solid (m. p. 171.2 – 173.4 °C). Assuming the product is 3,5-dimethylbenzoic acid, calculate the percent yield. Br 1) Mg°, Et,0 ОН 2) CO2 3) H* 1-bromo-3,5-dimethylbenzene…
Write an equation for the acid-base reaction between 2,4-pentanedione and sodium eth- oxide and calculate its equilibrium constant, K. The pK, of 2,4-pentanedione is 9; that of ethanol is 15.9. CH,CCHÖCH, + CH,CH,O Na* H 2,4-Pentanedione Sodium ethoxide
(a) Tsomane and Nyiko were given a task of synthesising methylenecyclohexane 2. After a brief discussion with each other, Tsomane proposed Method A to synthesise 2 from cyclohexanone 1 while Nyiko proposed Method B that started from hydroxymethylcyclohexane 3. Each student believed that their proposed method is better than the other. (Scheme below) (1) Ph Ph 8*8 Ph THF A 1 Santande B H₂SO4 100 °C 3 OH Using curly arrows, provide full mechanistic details accounting how methylenecyclohexane 2 was synthesised according to both Methods A and B.
1. In the reactions involving the three isomeric alcohols with the formula C4H9OH, describewhat each of the following tests showed about reactivity of the -OH group and reactions of 1°,2°, and 3° alcohols.• the test with neutral KMnO4• the test with concentrated HCl2. Predict how the fourth alcohol with the formula C4H10O would react if tested with:• 0.01 M KMnO4• concentrated HCl at room temperatureExtend FurtherUse your observations of the solutions formed in the previous experiments and yourunderstanding of alcohols to complete a table like the one shown below. Research the meltingand boiling points to verify your answers.