A. Calibration of pH probe (mark with check) B. Titration of HCI 1. M of NaOH (from bottle): 2. Volume of HCI: 25 0.100 pH = 4.0 D pH = 7.0 E pH=10.0 M mL = 0, 025 L == 3. moles of HCI (MHCI X VHCI, in L) = 4. Volume of NaOH at equivalence point: 2.5 moles 0.1/75 mL = L 5. M of NaOH (experimental) at equivalence point (moles NaOH = moles HCl(1/VolNaOH) = 6. pH at equivalence point: Volume NaOH (mL) pH reading Volume NaOH (mL) pH reading Volume NaOH (mL) pH reading 0.00 l 1.00 1.60 2.00 اما ١٠ 16.00 2.0 26.50 10.15 17.00 2.08 27.00 0.97 18.00 2.13 27.50 11.15 3.00 42 19.00 2,20 28.00 11.24 4.00 20.00 1.64 2.27 28.50 1.34 5.00 20.50 2.32 29.00 11.42 6.00 1.69 21.00 2.31 29.00 7.00 8.00 1.71 11:72 21.50 2.43 30.00 11.53 22.00 31.00 2.51 9.00 1.76 22.50 2.59 32.00 11.66 10.00 1.78 23.00 2.7 34.00 11.79 11.00 81 23.50 2.81 36.00 11.86 12.00 11.85 24.00 2.99 38.00 11.94 13 42.50 1.88 24.50 3.29 40.00 12.00 13.00 1.92 25.00 4.30 42.00 12.03 14.00 1.97 25.50 7,21 45.00 12,10 15.00 2.00 26.00 0.17 50.00 127

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter20: Applications Of Oxidation/reduction Titrations
Section: Chapter Questions
Problem 20.29QAP
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What is caculated pH at 0.00 mL of NaOH and Percentage error? Experiement pH 1.61

What is caculated pH at 12.50 mL of NaOH and Percentage error? Experiement pH is 1.85

What is caculated pH at 25.00  mL of NaOH and Percentage error? Experiement pH is 4.30

What is caculated pH at 30.00  mL of NaOH and Percentage error? Experiement pH is 11.53

 

A. Calibration of pH probe (mark with check)
B. Titration of HCI
1. M of NaOH (from bottle):
2. Volume of HCI: 25
0.100
pH = 4.0 D pH = 7.0 E pH=10.0
M
mL = 0, 025 L
==
3. moles of HCI (MHCI X VHCI, in L) =
4. Volume of NaOH at equivalence point:
2.5 moles 0.1/75
mL =
L
5. M of NaOH (experimental) at equivalence point (moles NaOH = moles HCl(1/VolNaOH) =
6. pH at equivalence point:
Volume NaOH (mL) pH reading Volume NaOH (mL) pH reading Volume NaOH (mL) pH reading
0.00 l
1.00
1.60
2.00
اما ١٠
16.00 2.0
26.50 10.15
17.00
2.08
27.00 0.97
18.00
2.13
27.50 11.15
3.00
42
19.00 2,20
28.00 11.24
4.00
20.00
1.64
2.27
28.50 1.34
5.00
20.50
2.32
29.00 11.42
6.00 1.69
21.00 2.31
29.00
7.00
8.00
1.71
11:72
21.50 2.43
30.00 11.53
22.00
31.00
2.51
9.00 1.76
22.50 2.59
32.00 11.66
10.00
1.78
23.00 2.7
34.00
11.79
11.00
81
23.50
2.81
36.00 11.86
12.00
11.85
24.00 2.99
38.00
11.94
13 42.50
1.88
24.50 3.29
40.00
12.00
13.00
1.92
25.00 4.30
42.00
12.03
14.00
1.97
25.50 7,21
45.00 12,10
15.00 2.00
26.00 0.17
50.00 127
Transcribed Image Text:A. Calibration of pH probe (mark with check) B. Titration of HCI 1. M of NaOH (from bottle): 2. Volume of HCI: 25 0.100 pH = 4.0 D pH = 7.0 E pH=10.0 M mL = 0, 025 L == 3. moles of HCI (MHCI X VHCI, in L) = 4. Volume of NaOH at equivalence point: 2.5 moles 0.1/75 mL = L 5. M of NaOH (experimental) at equivalence point (moles NaOH = moles HCl(1/VolNaOH) = 6. pH at equivalence point: Volume NaOH (mL) pH reading Volume NaOH (mL) pH reading Volume NaOH (mL) pH reading 0.00 l 1.00 1.60 2.00 اما ١٠ 16.00 2.0 26.50 10.15 17.00 2.08 27.00 0.97 18.00 2.13 27.50 11.15 3.00 42 19.00 2,20 28.00 11.24 4.00 20.00 1.64 2.27 28.50 1.34 5.00 20.50 2.32 29.00 11.42 6.00 1.69 21.00 2.31 29.00 7.00 8.00 1.71 11:72 21.50 2.43 30.00 11.53 22.00 31.00 2.51 9.00 1.76 22.50 2.59 32.00 11.66 10.00 1.78 23.00 2.7 34.00 11.79 11.00 81 23.50 2.81 36.00 11.86 12.00 11.85 24.00 2.99 38.00 11.94 13 42.50 1.88 24.50 3.29 40.00 12.00 13.00 1.92 25.00 4.30 42.00 12.03 14.00 1.97 25.50 7,21 45.00 12,10 15.00 2.00 26.00 0.17 50.00 127
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