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- A volumetric calcium analysis on triplicate samples of the blood serum of a patient believed to be suffering from a hyperparathyroid condition produced the following data: mmol Ca/L = 3.55, 3.65, 3.14. What is the 95% confidence interval for the mean of the data, assuming(a) No prior information about the precision of the analysis?(b) s → σ = 0.056 mmol Ca/L?In the Analytical Chemistry laboratory, one of the B.Sc student Ms. Fatma wanted to analyze the presence of Iron(II) ion in the water samples collected from Sohar Industrial Area in the Sultanate of Oman and analyzed by Spectrophotometric method. (1) 250.00 mL of this water sample (Solution A) known to contain unknown amount of FeSO4. She has diluted Solution A by a dilution factor 10 to make 250.00 mL solution, which she labeled Solution B. Using Spectrophotometer, she has measured the absorbance value (0.642) for Solution B at 508 nm using 1.00 cm cell (cuvet). The molar absorptivity value for Fe2* ion at 508 nm is ɛ508 = 30.8 M-1cm1. (i) What volume of the solution A did she require to make the 250.00 mL of Solution В? (ii) in (i)? What instrument should she use to transfer the volume of the Solution A calculated (ii) Concentration of FeSO4 in Solution B. (iv) Concentration of FeSO4 in Solution A. Mass of FeSO4 in Solution A (Show your calculation) (v)1. (a) A solution of NaCl is prepared by dissolving 0.0056 g NaCl with enough H2O in a volumetric flask to yield a final volume of 10 mL. Assuming a standard (0.1 mg) analytical balance and class A glassware is employed, calculate the concentration of the solution (M) and its corresponding error. The atomic weights of Na and Cl are 22.98976928(2) and 34.45(1), respectively (the number in parentheses indicating the error in the last digit). (b) What would the error be if a 1mL transfer pipet was employed (10x) rather than the 10 mL volumetric flask?
- A new analytic instrument is capable of detecting picogram quantities of a chemi-cal substance. How many times more capable is this instrument than one that candetect nanogram quantities of the same chemical?A volumetric calcium analysis on triplicate samples of the blood serum of a patient believed to be suffering from a hyperparathyroid condition produced the following data: mmol Ca/L = 3.15, 3.25, 3.26. What is the 95% confidence interval for the mean of the data, assuming no prior information about the precision of the analysis?(d) By using the data provided below, calculate the PillingBedworth ratio for the nickel (Ni) – nickel oxide (NiO) system and determine whether NiO is protective against corrosion. Atomic mass of nickel = 58.7 g.mol-1 Density of nickel = 8.91 Mg.m-3 Molecular mass of nickel oxide = 74.7 g.mol-1 Density of nickel oxide = 6.67 Mg.m-3 (e) A stainless steel pressure vessel that has fracture toughness, K1C, of 197 MN.m-3/2 is going to be exposed to a stress of 398 MN.m-2 . By using this information explain how designers can determine the thickness of the vessel so that catastrophic failure can be avoided.
- 3. (a) If 10.0 mL of H2SO4 (sp. Gr. 1.50, containing 48.7% of combined SO3 by weight) is diluted to 400 mL, what is the normality of the solution as an acid? (b) What volume of 6.00 M H2SO4 should be added to this in order to make the resulting mixture 1.00 N as an acid? FW's : H2SO4 = 98; SO3 = 80(2) In the Analytical Chemistry Laboratory Mr.Yahiya Al Moqbali wanted to prepare KCI solution. He has dissolved 2.634 (+0.002) g of KCI in a 250.00 (±0.08) mL volumetric flask. Calculate the molarity of the solution and express your answer with its absolute uncertainty and give reasonable number of significant figure. [The formula mass of KCI is 74.5513 (±0.001) amu] (Show your Calculation)2b) What is the primary consideration?
- (a) A solution of 20.91 % by weight H2SO4 has a specific gravity of 1.150. What is the normality of this solution? (b) Water is added to dilute this solution to a solution of 3.03% by weight H2SO4 (SG= 1.020). What is the new normality of the resulting solution and how were they mixed? (Assume 100 mL of the original solution was used.)professor Scimemi has accepted you as a Master’s student and you are involved in a project that studies the cellular basis of neuropsychiatric diseases. For your electrophysiology recordings you have to make a recording solution containing (in mM): 119 NaCl, 2.5 KCl, 2.5 CaCl2, 1 MgCl2, 26.2 NaHCO3, 1 NaH2PO4, 22 glucose. You need 800 ml of it. How much KCl do you need to weigh out? Hint: we only care about KCl here. (MW KCl is 74.55 g/molThe physical fitness of athletes is measured by “VO2 max,”which is the maximum volume of oxygen consumed by anindividual during incremental exercise (for example, on atreadmill). An average male has a VO2 max of 45 mL O2>kgbody mass/min, but a world-class male athlete can have a VO2max reading of 88.0 mL O2>kg body mass/min. (a) Calculatethe volume of oxygen, in mL, consumed in 1 hr by an averageman who weighs 185 lbs and has a VO2 max reading of 47.5mL O2>kg body mass/min. (b) If this man lost 20 lb, exercised,and increased his VO2 max to 65.0 mL O2>kg body mass/min,how many mL of oxygen would he consume in 1 hr?