Caffeine occurs naturally in tea leaves and coffee beans. Pure caffeine (mp 236°C) is a white crystalline solid material at room temperature. It is classified as an alkaloid - a nitrogen-containing basic compound that is obtained from plants and has physiological effects in the body. A student pulverizes 8.78 grams (g) of coffee beans into a finely ground powder by using a mortar and pestle. The caffeine is then extracted into 300 mL of boiling dichloromethane (CH2CII2) by the same solid- liquid extraction technique used in Unit 1. After 30 minutes, the solution is filtered hot to remove a large amount of brown insoluble material. Dichloromethane is removed from the filtrate via rotary evaporation, leaving 916.3 milligrams (mg) of caffeine behind, as a white solid. What is the percentage of isolated caffeine with respect to the starting amount of crude coffee beans?

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ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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Caffeine occurs naturally in tea leaves and coffee beans. Pure caffeine (mp 236°C) is a white
crystalline solid material at room temperature. It is classified as an alkaloid - a nitrogen-containing
basic compound that is obtained from plants and has physiological effects in the body. A student
pulverizes 8.78 grams (g) of coffee beans into a finely ground powder by using a mortar and pestle.
The caffeine is then extracted into 300 mL of boiling dichloromethane (CH2CI2) by the same solid-
liquid extraction technique used in Unit 1. After 30 minutes, the solution is filtered hot to remove a
large amount of brown insoluble material. Dichloromethane is removed from the filtrate via rotary
evaporation, leaving 916.3 milligrams (mg) of caffeine behind, as a white solid. What is the percentage
of isolated caffeine with respect to the starting amount of crude coffee beans?
caffeine
Transcribed Image Text:Caffeine occurs naturally in tea leaves and coffee beans. Pure caffeine (mp 236°C) is a white crystalline solid material at room temperature. It is classified as an alkaloid - a nitrogen-containing basic compound that is obtained from plants and has physiological effects in the body. A student pulverizes 8.78 grams (g) of coffee beans into a finely ground powder by using a mortar and pestle. The caffeine is then extracted into 300 mL of boiling dichloromethane (CH2CI2) by the same solid- liquid extraction technique used in Unit 1. After 30 minutes, the solution is filtered hot to remove a large amount of brown insoluble material. Dichloromethane is removed from the filtrate via rotary evaporation, leaving 916.3 milligrams (mg) of caffeine behind, as a white solid. What is the percentage of isolated caffeine with respect to the starting amount of crude coffee beans? caffeine
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