Carbonyl IR peaks are strong and sharp, so examining shifts in carbonyls can be telling of changes in the environment around that functional group. Citing your IR spectrum, comment on any evidence the esterification reaction was successful.

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter25: Instruments For Optical Spectrometry
Section: Chapter Questions
Problem 25.20QAP
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Carbonyl IR peaks are strong and sharp, so examining shifts in carbonyls can be telling of changes in the environment around that functional group. Citing your IR spectrum, comment on any evidence the esterification reaction was successful.

% Transmittance
100
% Transmittance
90
80-
70-
- 09
50-
40-
30
20-
10-
0
4000
LIQUID
95-
90
85
- 08
75-
70-
65
-09
55-
50-
45
40-
4000
UNKNOWN B
3500
3500
3000
www
3000
2500
2500
2000
Wavenumbers (cm-1)
2000
Wavenumbers (cm-1)
mwn
1723.20
1500
1684.59
1676.05
1452.72
1500
1323.07
1275.37
1419.93
1110.20
Klongher
1288.38
1070.77
1082.54
1000
1000
709.79
931.11
683.46
500
665.82
542.67
500
Transcribed Image Text:% Transmittance 100 % Transmittance 90 80- 70- - 09 50- 40- 30 20- 10- 0 4000 LIQUID 95- 90 85 - 08 75- 70- 65 -09 55- 50- 45 40- 4000 UNKNOWN B 3500 3500 3000 www 3000 2500 2500 2000 Wavenumbers (cm-1) 2000 Wavenumbers (cm-1) mwn 1723.20 1500 1684.59 1676.05 1452.72 1500 1323.07 1275.37 1419.93 1110.20 Klongher 1288.38 1070.77 1082.54 1000 1000 709.79 931.11 683.46 500 665.82 542.67 500
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