Chem 105 Online Post Laboratory Questions: Boo 20550 ante 1. What is the purpose of rinsing the precipitate at the end of the reaction? How would your calculation for percent yield be affected if this were not rinsed thoroughly? OBJECT In t

Fundamentals Of Analytical Chemistry
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Chapter7: Statistical Data Treatment And Evaluation
Section: Chapter Questions
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Please help with question 1
of prelab (see
tion. You may also
I solution stays in
overfill the
has a uniform
umber 2 of prelab
ed cylinder.
tion. You may also
solution stays in
overfill the
as a uniform
mass for the second
0.250M CaCl2 into
a graduated
measuring a new
1. The mixture will
This Photo by Unknown Author is licensed un
pernatant until it is
passes.
itate a few times
Ditate. This ensures
Chem 105 Online
that all the spectator ions are rinsed off the filter paper and precipitate and not
recrystallize-which would add an additional mass on the filter paper when dried.
7. Carefully remove the filter paper (it will still be very moist) and place it on a paper towel
to dry overnight.
a. If you are cramped for time, an oven will work set at 200-225°F. Set the wet filter
paper on a baking sheet and place in the oven. Check it regularly to not burn
the filter paper.
b. A sunny window is a happy medium for wet filter paper as well. Ⓒ
8. Repeat the process one more time for a second trial. This time you will measure 10.0mL
of 0.750M Na2CO3 and 50.0mL of 0.250M CaCl₂ into a new plastic cup..
Don't forget your documentation!
Data Table
Data Entry
Quantities Used
Theoretical Yield of
Precipitate (record
here, show calculations
below table)
Mass of Filter Paper
BEFORE experiment
Mass of DRY Filter Poper
and Precipitate (day 2)
Mass of Calcium
Carbonate
(Precipitate, day 2)
Percent Yield
Trial 2
Trial 1
30.0mL of 0.250M CaCl₂
15.0mL of 0.750M Na2CO3
.53g
Trial 2
50.0mL of 0.250M CaCl2
10.0mL of 0.750M Na2CO3
.53g
Calculations
For each trial, show the theoretical yield of Calcium Carbonate produced based on your limiting
reactant and amounts of each reactant used.
Trial 1
Cat
Naz
Transcribed Image Text:of prelab (see tion. You may also I solution stays in overfill the has a uniform umber 2 of prelab ed cylinder. tion. You may also solution stays in overfill the as a uniform mass for the second 0.250M CaCl2 into a graduated measuring a new 1. The mixture will This Photo by Unknown Author is licensed un pernatant until it is passes. itate a few times Ditate. This ensures Chem 105 Online that all the spectator ions are rinsed off the filter paper and precipitate and not recrystallize-which would add an additional mass on the filter paper when dried. 7. Carefully remove the filter paper (it will still be very moist) and place it on a paper towel to dry overnight. a. If you are cramped for time, an oven will work set at 200-225°F. Set the wet filter paper on a baking sheet and place in the oven. Check it regularly to not burn the filter paper. b. A sunny window is a happy medium for wet filter paper as well. Ⓒ 8. Repeat the process one more time for a second trial. This time you will measure 10.0mL of 0.750M Na2CO3 and 50.0mL of 0.250M CaCl₂ into a new plastic cup.. Don't forget your documentation! Data Table Data Entry Quantities Used Theoretical Yield of Precipitate (record here, show calculations below table) Mass of Filter Paper BEFORE experiment Mass of DRY Filter Poper and Precipitate (day 2) Mass of Calcium Carbonate (Precipitate, day 2) Percent Yield Trial 2 Trial 1 30.0mL of 0.250M CaCl₂ 15.0mL of 0.750M Na2CO3 .53g Trial 2 50.0mL of 0.250M CaCl2 10.0mL of 0.750M Na2CO3 .53g Calculations For each trial, show the theoretical yield of Calcium Carbonate produced based on your limiting reactant and amounts of each reactant used. Trial 1 Cat Naz
3
C
Chem 105 Online
Post Laboratory Questions:
broshan
1. What is the purpose of rinsing the precipitate at the end of the reaction? How would
your calculation for percent yield be affected if this were not rinsed thoroughly?
2. Suppose a student introduces an object to aid in stirring the solution but does not rinse
the object and places it directly on their countertop. They notice a white powder that
resides on the stirrer. How will their calculation for percent error be affected? Explain.
The percent error would be incorrect because
we wouldn't
3. Why must the filter paper be dried before obtaining the final mass?
4. Would you classify this process as an effective method to form Calcium Carbonate?
What are the limitations of the experiment if it were to be done on a commercial level?
What changes would you make if you needed to perform this in a commercial setting?
Chem 10
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Transcribed Image Text:3 C Chem 105 Online Post Laboratory Questions: broshan 1. What is the purpose of rinsing the precipitate at the end of the reaction? How would your calculation for percent yield be affected if this were not rinsed thoroughly? 2. Suppose a student introduces an object to aid in stirring the solution but does not rinse the object and places it directly on their countertop. They notice a white powder that resides on the stirrer. How will their calculation for percent error be affected? Explain. The percent error would be incorrect because we wouldn't 3. Why must the filter paper be dried before obtaining the final mass? 4. Would you classify this process as an effective method to form Calcium Carbonate? What are the limitations of the experiment if it were to be done on a commercial level? What changes would you make if you needed to perform this in a commercial setting? Chem 10 OBJECT In t СОГ CO BACKG Che On mc Spe ter me ab Ta CO C Er te W I (
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