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- TLC, a powerful analytical tool, can be used to monitor the progress of reactions. The synthesis of ethyl-3-coumarincarboxylate can be monitored by TLC by displaying the starting aldehyde 1, and coumarin product 2, which have very distinct Rf values (Hint: Think about the polarity of compounds 1 and 2 in terms of their abilities to H-bonds to silica gel). What can be determine about the progress of the reaction from analysis of the TLC shown below?What is the organic product(s) expected when this compound undergoes the Simmons-Smith reaction.Briefly explain why the Suzuki reaction can take place in aqueous solution whereas a Grignardreaction requires anhydrous conditions.
- Why is it difficult to stop the reaction at the mono-brominated stage?This reaction also produces diacetylferrocene. However, this compound remains near the top of the column. Explain why this is so and what you could do to elute it. Explain the order of elution of fer- rocene, acetylferrocene, and diacetylferrocene.a) Write down the products that will occur when you withdraw HBr from 2-bromine-3-methyl butane in a basic medium, State the reaction conditions. Show which product is the main product. b) Does the main product show the geometric isomer, so please write together. If it shows write the isomers. c) Write the product that will be formed when the main product reacts with KMnO4 in a basic environment in cold.
- Compare acetanilide, which was in the recrystallization lab and acetaminophen (2) shown below. Which compound do you predict would have a larger Rf value? Briefly explain in less than 10 words.why it is not a good idea to use dichloromethane as a solvent in Grignard reactions.At the start of lab, Anthony adds vanillin to his Erlenmeyer flask, then adds sodium hydroxide, and lets the suspension cool. i. With minimal words, identify the reaction that takes place between sodium hydroxide and vanillin. ii. Is sodium borohydride capable of inducing the same reaction as (i)? Explain.
- Usually the aqueous layer is extracted multiple times with organic. This is more common during a certain lab experiment but in the synthesis of n-Hexyl acetate reaction the organic layer is extracted multiple times with water. why we have to do it this way for this specific reaction?Compare the function of the solvent (methanol) in the E1 and SN1 reactions.what would a detailed step-by-step mechanism be for a reaction between bromine and trans-stilbene if the solvent, ethanol, is a stronger nucleophile than the bromide ions?