IR Spectrum (liquid film) 4000 100 80 8 8 8 8 % of base peak 60 40 20 3000 40 10 13C NMR Spectrum (500 MHz, CDCI, solution) 73 200 80 proton decoupled ¹H NMR Spectrum (200 MHz, CDCI, solution) 45 9 exchanges with D₂0 DEPT CH₂ CH, CHI J M 1720 40 2000 8 138 116 V (cm¹) 140 120 160 m/e 1600 L 160 expansions ì 20 L 7 1200 M+ 194/198 (<1%) 120 Mass Spectrum 240 200 ill 6 C6H₁10₂Br 280 800 1.0 ppm 5 solvent 1 1 80 1 4 No significant UV absorption above 220 nm 40 L 3 1 2 08 (ppm) 1 TMS 0 8 (ppm)
IR Spectrum (liquid film) 4000 100 80 8 8 8 8 % of base peak 60 40 20 3000 40 10 13C NMR Spectrum (500 MHz, CDCI, solution) 73 200 80 proton decoupled ¹H NMR Spectrum (200 MHz, CDCI, solution) 45 9 exchanges with D₂0 DEPT CH₂ CH, CHI J M 1720 40 2000 8 138 116 V (cm¹) 140 120 160 m/e 1600 L 160 expansions ì 20 L 7 1200 M+ 194/198 (<1%) 120 Mass Spectrum 240 200 ill 6 C6H₁10₂Br 280 800 1.0 ppm 5 solvent 1 1 80 1 4 No significant UV absorption above 220 nm 40 L 3 1 2 08 (ppm) 1 TMS 0 8 (ppm)
Organic Chemistry
8th Edition
ISBN:9781305580350
Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Publisher:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Chapter14: Mass Spectrometry
Section: Chapter Questions
Problem 14.37P
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Provide the structure of the molecule that would give rise to these spectra. Include degree of unsaturation, functional groups present, assignment of 1H and 13C NMR peaks by labeling each peak with specific atoms in the structure (a,b,c,d) and show which atoms give rise at which peaks
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