mass of unknown crude for acid and neutral is 0.03 grams mass of unknown recrystallized for acid and neutral is 0.03 grams. I need help in finding overall percent

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter20: Applications Of Oxidation/reduction Titrations
Section: Chapter Questions
Problem 20.6QAP
icon
Related questions
Question
mass of unknown crude for acid and neutral is 0.03 grams mass of unknown recrystallized for acid and neutral is 0.03 grams. I need help in finding overall percent
Experiment 3
Using acid-base extraction to separate a mixture
Assuming that your unknown mixture is composed of exactly 50% acid compound and
50% neutral compound, complete the table below. Show all calculations - you may
handwrite your calculations.
Note: "overall percent recovery" compares how much of each component you started with
in the mixture to the final mass obtained after recrystallization. In addition, 30 mg of crude
compound was reserved prior to recrystallization and should be accounted for in some way
when calculating the overall percent recovery of the compound from the mixture.
Mass of
Percent recovery
from extraction
Overall percent
Mass of
Compound
crude pdt
recryst'd pdt
recovery
unknown
acid
unknown
neutral
Based on your melting point ranges of your crude products as well as the appearance of the
TLC plates for your crude products, was recrystallization necessary to purify your acid
and/or neutral product? Why or why not? Explicitly include all relevant data for each
component of your answer.
Hint: the difference in the two temperatures of a melting point range tells you something
important about the purity of the compound.
BecrystallizationYG no eceSSoV c SO Onmelting peint only
Transcribed Image Text:Experiment 3 Using acid-base extraction to separate a mixture Assuming that your unknown mixture is composed of exactly 50% acid compound and 50% neutral compound, complete the table below. Show all calculations - you may handwrite your calculations. Note: "overall percent recovery" compares how much of each component you started with in the mixture to the final mass obtained after recrystallization. In addition, 30 mg of crude compound was reserved prior to recrystallization and should be accounted for in some way when calculating the overall percent recovery of the compound from the mixture. Mass of Percent recovery from extraction Overall percent Mass of Compound crude pdt recryst'd pdt recovery unknown acid unknown neutral Based on your melting point ranges of your crude products as well as the appearance of the TLC plates for your crude products, was recrystallization necessary to purify your acid and/or neutral product? Why or why not? Explicitly include all relevant data for each component of your answer. Hint: the difference in the two temperatures of a melting point range tells you something important about the purity of the compound. BecrystallizationYG no eceSSoV c SO Onmelting peint only
Expert Solution
trending now

Trending now

This is a popular solution!

steps

Step by step

Solved in 2 steps

Blurred answer
Similar questions
  • SEE MORE QUESTIONS
Recommended textbooks for you
Fundamentals Of Analytical Chemistry
Fundamentals Of Analytical Chemistry
Chemistry
ISBN:
9781285640686
Author:
Skoog
Publisher:
Cengage