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- Complete the following reaction scheme. 1. DIBALH 2. H3O+ TMSCI Pyridine 1. LIAIH(t-BuO)3 SOCI2 2. H3O+ CrO3 H3O+Q5. A. Complete the incomplete reactions. Also write stepwise mechanism for the given reactions. CH3 i. BH3, THE ii. H2O2, HO Br H20 ii. H3C OH H. H3C Br Br2, H20 CH3 Br OH organic solvent CH3 КОН CI V. + CHCI3 KCI CIProvide a plausible arrow pushing mechanism for the reaction below. Os-OtBu 's-OtBu HN 1. LDA 2. OMe SO,Ph 3. aqueous workup
- In the boxes below, enter the LETTER for the reagents needed in each step to complete the following an A. H₂O, H₂O+ B. HgSO4, H₂SO4, H₂O C. CH₂CH₂Br D. KOC(CH3)3 Step 1 E. NaNH,, NH F. Na, NH3 G. 1) Sia₂BH 2) H₂O₂, NaOH H. CH3CH₂CH₂Br Step 2 J. NaOH K. CH₂CH₂CH₂CH₂Br L.H₂, Lindlar catalyst Step 3Identify the correct first mechanism step and final product of the reaction shown. 1. ВНз, THF 2. Н2О2, ОН" mechanism step final product H-BH2 OH А. H-BH2 H-BH2 OH C. H-BH2 LBH2 D. OH B.Draw the major product of this reaction. Ignore inorganic byproducts. 1. Hg(OAc)2, H₂O 2. NaBH4, NaOH Drawing at
- Provide the missing compounds and reagents in the reaction scheme. Identify reagent 5. OH reagent 2 reagent 1 H2SO4 но Compound 1 (conc.) 1) BH3 2) H,O, H,SO, (conc.) NaOH, H2O reagent 3 CrO3, H* A Compound 4 NABH4 1) O3 2) Zn, H;O* reagent 5 reagent 4 H,SO4 Compound 3 Compound 2 1) CH;MgBr (conc.) 2) H;O+ Identify reagent 1. Identify reagent 2. Identify reagent 3. Identify reagent 4. 1) CH3MGB1 2) H;O* H,SO̟ (conc.) H,SO, (conc.) H,SO, (conc.) CrO3, H+ 1) ВН, NaBH4 1) O3 NaBH, 2) H2O2 2) Zn, H3O* 1) CH,MgBr 1) BH3 NaBH, 2) H3O+ NABH, 2) H,O2 1) CH;MgBr 1) O3 1) BH3 1) O3 2) Zn, H3O* 2) H;0* 2) Zn, H,O+ 2) H,O2 1) O3 CrO3, H+ CrO3, H+ H,SO4 (conc.) 2) Zn, H,O* 1) CH; MgBr 2) H,0* 1) ВН, CrO3, H* 2) H,O,Q4. The herbicide oxyfluorfen can be prepared by the reaction between phenol and an aryl fluoride. Propose a curved arrow mechanism for this reaction. 1 F3C. LOCH2CH3 F3C. КОН CI `NO2 CI OH LOCH2CH3 `NO2 Oxyfluorfen2. Provide the product of each of the following reactions or reaction sequences. H H H Br. Br H H H 1. xs NaNH, 2. EtCl 3. H₂, Lindlar's catalyst 1. NaNH2 2. Mel 3. 9-BBN 4. 202, NaOH 1. NaNH, 2. Mel 3. H₂SO4, H₂O, HgSO4 1. NaNH, 2. Mel 3. NaNH, 4. Etl 5. Na, NH3 1. Br₂ 2. XS NaNH2 3. Etl 4. H₂, Lindlar's catalyst 2
- Provide a plausible arrow pushing mechanism for the reaction below. 1. ABULI ŅME2 2. MgCl HO,C, 3. CO2 4. acidic workup F NME2 NME2Provide the missing intermediates and final product in the following synthesis. 1. LDA (excess). A 2. Н,о Br2 1. NaH В 2. C H,/Pd CI4 Lindlar catalyst ВА 1. CH,MgBr H,CrO4 D E 2. NH,CI, H,O F G7. Mechanism Draw a complete arrow-pushing mechanism for the following reaction. in H NaBH3CN H₂SO4 (dilute) ~_~_^ non