some components of clove oil eugenol eugenol acetate B-caryophyllene HO clove oil hexanes (50 mL) NaOH (25 mL, 5% aq) aqueous organic NAOH (10 mL, 5% aq) 1) dry with Na2SO4 2) gravity filter 3) remove solvent on rotovap combine aqueous layers conjugate base of eugenol here neutral organic aqueous compounds Figure 9: separation of eugenol from the less acidic components of clove oil by acid/base extraction

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter31: Introduction To Analytical Separations
Section: Chapter Questions
Problem 31.19QAP
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Starting from crude clove oil, draw flow charts to illustrate the extraction steps.

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some components of clove oil
eugenol
eugenol acetate
B-caryophyllene
H.
HO
clove oil
hexanes (50 mL)
NaOH (25 mL, 5% aq)
aqueous
organic
NaOH (10 mL, 5% aq)
1) dry with Na2SO4
2) gravity filter
3) remove solvent
on rotovap
combine
aqueous
layers
conjugate base of
eugenol here
0.
neutral
organic
aqueous
compounds
Figure 9: separation of eugenol from the less acidic components of clove oil by acid/base extraction
Transcribed Image Text:some components of clove oil eugenol eugenol acetate B-caryophyllene H. HO clove oil hexanes (50 mL) NaOH (25 mL, 5% aq) aqueous organic NaOH (10 mL, 5% aq) 1) dry with Na2SO4 2) gravity filter 3) remove solvent on rotovap combine aqueous layers conjugate base of eugenol here 0. neutral organic aqueous compounds Figure 9: separation of eugenol from the less acidic components of clove oil by acid/base extraction
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