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- C. Nickel in a sample was determined using a new procedure where six replicate samples resulted in a mean of 19.65% and a variance of 0.4524. Five replicate analyses where conducted using a standard procedure resulting in a mean of 19.24% and a variance of 0.105. If the pooled standard deviation was +0.546, is there a significant difference between the two methods?2. A gas chromatogram of a four-(4)-component mixture had the following areas and retention times (RT). Component ABCD (RT) (min) 2.564 5.241 1.904 3.217 Area (mm²) 2341 1278 4302 1987 A. Which compound do you suspect is the most volatile? Why? B. Calculate the percent composition of component D.Can paper chromatography be used to separate and identify very volatile substances? How do I prove this.
- Sample IdentificationCodeConcentration of M%TA=2-log(%T)Q50004.00 x 10-417.90.75Q50013.20 x 10-425.00.6Q50022.40 x 10-435.70.46Q50031.60 x 10-450.20.3Q50048.000 x 10-570.80.15SampleIdentificationCode%TA=2-log(%T)AMQ0210150143.70.359518560.360.000192Q0210150244.10.355561410.360.00018Q0210150343.80.358525890.360.00017Q0210150444.10.355561410.360.00018Q0210150543.80.358525890.360.00017What was their percent error?43%Does Batch 021015 meet legal requirements?No, because it is not between 2.85 * 10(4) and 3.15 * 10(4)Well #DropsBluedye1234567891012345678910Drops 9Distilled water876543210Concne 0.26tration0.52Test Tube #0.781.041.3Solutions3Concentration (M)2.082.32.6Concentration (ppm)1:1 dilution11.82Starting Dilution21.562:1 dilution0A.Zero standard0Was your calibration curve as linear as you expected?B.Did you experience any âdriftâ of the resistance readings?C.What is the equation of your best-fit line?D.What commercial drink did you analyze?E.Assuming…One disadvantage of thin layer chromatography is that... it cannot be used for quantitative measurements. O it consumes large volumes of solvents O it cannot analyze volatile samples it cannot be used to analyze many samples simultaneously it requires a large amount of sample for analysisWhich technique is based on the stronger attractionsome components have for the stationary phasecompared to the mobile phase? A. filtration D. chromatographyB. distillation E. sublimationC. crystallization
- The following data give the recovery of bromide from spiked samples of vegetable matter, measuredusing a gas–liquid chromatographic method. The same amount of bromide was added to each specimen(Roughan, J.A., Roughan, P.A. and Wilkins, J.P.G., 1983, Analyst, 108: 742).Tomato: 777 790 759 790 770 758 764 ug/gCucumber: 782 773 778 765 789 797 782 ug/g(a) Test whether the recoveries from the two vegetables have variances which differ significantly.(b) Test whether the mean recovery rates differ significantly.You have obtained a gas chromatogram of a two component mixture of compounds A and B. The height of peak A is 3.84 cm. and the width at half height is 1 cm. The height of peak B is 3.49 cm. and the width at half height is 1.36 cm. The percentage of a component in the mixture is proportional to peak area. Estimate peak areas by multiplying height by width at half height. What was the percentage of compound B in the mixture? (Enter your answer as a number without any percent symbol or the word percent.)How does paper chromatography allow you to separate substances?
- One method for quantitative determination of the concentration of constituents in a sample analyzed by gas chromatography is the area normalization method. In this method, complete elution of all of the sample constituents is necessary. The area of each peak is then measured and corrected for differences in detector response to the different eluates. This correction is accomplished by dividing the area by an empirically determined correction factor. The concentration of the analyte is found from the ratio of its corrected area to the total corrected area of all peaks. For a chromatogram containing three peaks, the relative areas were found to be 16.4, 45.2, and 30.2 in the order of increasing retention time. Calculate the percentage of each compound if the relative detector responses were 0.60, 0.78, and 0.88, respectivelyIn chromatography, it is desirable to increase the resolution. a) increase the plate height (H) b) decrease the plate height (H) c) decrease the number of plates (N) toIn chromatography the concentration of a separated compound is directly related to a) stationary phase concentration b) absorbance c) wavelength d) peak area