As a group, use your knowledge of acid-base extraction to come up with a plan to separate the following compounds from each other. Your plan should include specific solvents or reagents to be used and result in 4 isolated solids in the end. p-anisidine pyrene salicylic acid 2,3-xylenol

As a group, use your knowledge of acid-base extraction to come up with a plan to separate the following compounds from each other. Your plan should include specific solvents or reagents to be used and result in 4 isolated solids in the end. p-anisidine pyrene salicylic acid 2,3-xylenol

Organic Chemistry

8th Edition

ISBN:9781305580350

Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote

Publisher:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote

Chapter23: Amines

Section: Chapter Questions

Problem 23.32P: Suppose you have a mixture of these three compounds. Devise a chemical procedure based on their...

See similar textbooks

Related questions

Q: Starting with benzene, give a sequence of laboratory reactions which could be used to prepare…

Q: Eugenol is a natural product derived from the dried flower buds of the evergreen tree, Eugenia…

A: Eugenol is a member of allylbenzenes with molecular formula C10 H12 O2. It is mostly extracted from…

Q: A mixture of compounds is dissolved in ether, and extracted with 10% NaHCO3 solution. The aqueous…

A: If the mixture contain amines, then it will be at the bottom layer of second extraction.

Q: A mixture is made up of low molecular weight carboxylic acid, alcohol and ester. What one step…

A: Extraction is the method to separate components from mixture

Q: Which of the following extractions would involve a gas being generated? extraction of acetic acid…

A: When a reaction is completed , mostly the solution does not contain the desired product, but also…

Q: Describe how to separate benzoic acid from p-dichlorobenzene using acid base extraction with water…

Q: rite the Method used in recrystallisation of benzoic acid, azobenzene, and p-nitroaniline

A: Answer - Recrystallisation - Recrystallization, also known as fractional crystallization, is a…

Q: A student was performing an acid-base extraction of a mixture of three compounds. The three…

A: The solution is as follows:

Q: 1. Melting point technique 2. Recrystallization technique| 3. Extraction (understand how to separate…

A: As per the guideline, since you have asked multiple questions, we have solved the first question for…

Q: Account for the greater amount of internal pressure in the aspirin extraction versus the ß- naphthol…

A: Given solution contain napthalene, B- naphthol and aspirin. Napthalene is a hydrocarbon and it's…

Q: you plan to carry out the syn- thesis of aspirin (acetylsalicylic acid) by reacting salicylic acid…

Q: Which method or methods can you use to obtain pure ethanol from ethanol-water mixture and to obtain…

A: i) To obtain pure ethanol from the ethanol-water mixture. ii) To obtain limonene from the lemon.

Q: Acetic acid, salicylic acid, benzoic acid all of them undergo esterification test separately with…

A: When carboxylic acid reacts with alcohol in presence of H2SO4 then ester is formed. Mechanism : At…

Q: ind the molecular formula of alkyne which contains 12.19% by mass of hydrogen. Alkyne has the…

A: b) Acts with silver ammonia solution indicates there is a terminal alkyne in the molecule.

Q: Andrea and Yvette are going to cook the most delicious food that ever going to exist for their tired…

A: Sugar is sucrose, a molecule consisting of 12 atoms of carbon, 22 atoms of hydrogen, and 11 atoms of…

Q: Preparation of para-iodonitrobenzene 1. Weight of p-nitroaniline = 0.552 g 2. Weight of…

A: Please find the attached sheet.

Q: The difference in melting points between trans-oleic acid (18:1,D9)(44.5C) and cis-oleic acid…

A: given data is trans-oleic acid (18:1,D9) melting point is (44.50C) cis-oleic acid melting point is…

Q: Treatment of salicylaldehyde (2-hydroxybenzaldehyde) with bromine in glacial acetic acid at 0°C…

Q: Alkene can be prepared from alcohol using acid catalyzed dehydration reaction a. Draw and label the…

Q: You have an organic acid, organic base, and a neutral organic compound all together in a solid…

A: The above example is acid base extraction example.

Q: Starting with cyclohexanol, give a sequence of laboratory reaction which could be used to produce…

A: Interpretation - Give a equence of laboratory reaction which could be used to produce cyclohexane…

Q: A colorless liquid, C4H6O, having a boiling point of 97-98°C was found to be soluble in water and…

A: Given the data for the unknown compound is: C4H6O is a colorless liquid and the boiling point is…

Q: . Explain the concept of Azeotropic distillation for the separation of Acetone, chloroform with neat…

A: An azeotrope or a constant boiling point mixture is a mixture of two or more liquids whose…

Q: Why are alcohols usually bad electrophiles? You must support your answer with data on the…

Q: Which of the following compounds would be the most soluble in H0 during extraction purification? A.…

A: ✓It has been found that {\rm{p}}{{\rm{K}}_{\rm{a}}}pKa value of 2- chlorobutanoic acid is lower…

Q: Which of the following extractions would involve a gas being generated? extraction of acetic acid…

A: Introduction to exraction : When a reaction is completed , mostly the solution does not contain the…

Q: If you had a mixture of the three compounds below, and wish to separate them by liquid-liquid…

A: It is a practical thing. Here our am is to separate the turnery organic mixture.

Q: Nitroethylene, HyC = CHNO, is a sensitive compound that must be prepared with great care. Attempted…

A: The low recovery of product & a white coating on the inner walls of the distillation apparatus…

Q: Context: Synthesis of Methyl Salicylate from Salicylic Acid In the liquid-liquid extraction of the…

A: A question based on analytical separations that is to be accomplished.

Q: 2- Which distillation technique(s) can be used for the purification of following mixtures? (bp of…

A: Different purification methods are present for organic compounds. The general methods of…

Q: If you began an experiment with 5.9 mL of benzyl alcohol and isolated 5.5 mL of the benzoic acid…

A: The percent yield for the experiment is to be determined from the given data. Given: volume of…

Q: It is desired to prepare polyester with the number average molecular weight, Mn 5000 g/mol by…

Q: Describe how functional groups (toluene to be specific) are characterized for the Nitration test and…

A: The remarkable stability of the unsaturated hydrocarbon benzene has been discussed in an earlier…

Q: 4. You are given a mixture of sodium benzoate and cyclohexylammonium chloride (structures below)…

A: Sodium benzoate and cyclohexylammonium chloride are first dissolved in water and add some organic…

Q: Given the balanced reaction between salicylic acid (C7H603) and acetic anhydride (C4H6O3) to produce…

A: The excess of reagent can be calculated from the balanced chemical reaction.

Q: 1. Explain what will happen to the (i) yield and (ii) purity, of aspirin if the following steps were…

A: Aspirin is a drug used for pain, fever and inflammation. Aspirin is a derivative of salicylic acid,…

Q: acidity:ethanol,ethylene glycol, acetic acid, 2,4-pentanedione,oxalic acid solid

A: Acid is substance which release hydrogen ions and base is a substance which abstract hydrogen from…

Q: where you have to construct the carbon chain. c) Write out 3 preparations of 2-methylpropanoic acid,…

A: The answer is as follows:

Q: Lipids from an organic sample are extracted separately using acetone (A), hexane (H), and ethanol…

Q: Describe some observations you found fascinating. Discuss the purpose of acquiring a melting point…

A: Given : Structure of acetylsalicylic acid. To find : Two major functional groups in acetylsalicylic…

Q: What is your observation if you differentiate 2-butanone and 2-methylbutanal using Tollen's reagent…

A: Tollen's Test It is used to distinguish between Aldehyde and ketones. It is also known as the silver…

Q: CLOVES co-distillation E14A.3 distillate: water + essential oil residue tert-butyl methyl ether…

A: Given extraction of eugenol from clove oil. Identify the IR peak associated with each functional…

Q: Compounds with 5 carbons or less and containing either oxygen, nitrogen or sulfur. Increasing the…

A: Introduction: We have to predict the solubility group.

Q: The hydrocarbon fluorene was treated with potassium t-butoxide in an acid-base reaction

A: Fluorene is a non aromatic compound, which easily remove a proton in form of H+ to form fluorenide…

Q: Use the space provided below to draw a flow chart showing how you could separate a mixture…

A: The flow chart for the extraction of given compounds has been shown below:

Q: Give results and explanation for what is chemically happening in the following reactions. A.…

A: Given reactions: A. Dehydration of Sucrose with Acid. B. Dehydration of Cellulose with acid. C.…

Question

p-anisidine
pyrene
salicylic acid
2,3-xylenol

Expert Solution

This question has been solved!

Explore an expertly crafted, step-by-step solution for a thorough understanding of key concepts.

This is a popular solution!

SEE SOLUTION Check out a sample Q&A here

Step 1-Introduction

VIEW

Step 2-Separation of the compounds

VIEW

Trending now

This is a popular solution!

Step by step

Solved in 2 steps with 1 images

SEE SOLUTION Check out a sample Q&A here

Knowledge Booster

Learn more about

Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.

Similar questions

Suppose you have a mixture of these three compounds. Devise a chemical procedure based on their relative acidity or basicity to separate and isolate each in pure form.
Show how to bring about each step in this synthesis of the herbicide propranil.
3. How would you separate these three molecules from one another utilizing acid/base extractions and ethyl acetate as your organic layer? You can use 10% HC1 (aq.), 10% NaOH (aq.), and 30% NaHCO3 (aq.) as your acids and bases. NH2 HO HO, OH OH ÓH OH
Phenols are less acidic than carboxylic acids, with values of pKa around 10. Phenols aredeprotonated by (and therefore soluble in) solutions of sodium hydroxide but not by solutions of sodium bicarbonate. Explain how you would use extractions to isolate the three purecompounds from a mixture of p-cresol (p-methylphenol), cyclohexanone, and benzoic acid.
You could extract caffeine from neutral organics by treatment with aqueous HCl (acid). Write the structure of the conjugate acid of caffeine (after treatment with HCl) and explain why it would dissolve in the aqueous layer.
Q2) Write a reaction for the following, with explanation. part 1) Dimethyl ketone with Hydrogen cyanide (HCN) part2) Preparation of M. nitro chlorobenzene from benzene, using nitric acid Sulfuric acid, Chlorine, AICI, and any reagent you need. part3) Solvation of ethylene epoxide in acidic medium
Q1/ Solid compounds (A) with the formula C13H100. Soluble in H2SO4 (conc.). Burn with black smoke and leave a trace . Compounds (A) give positive test with Baradays Reagent and negative result with chromic acid test. Give the structure of compound (A) with chemical equation.
Synthetize 3-phenyl-2-propenoic acid from benzaldehyde using whatever organic/inorganic reagents are needed. 3-phenyl-2-propenoic = 3-phenylacrylic acid
(a) Tsomane and Nyiko were given a task of synthesising methylenecyclohexane 2. After a brief discussion with each other, Tsomane proposed Method A to synthesise 2 from cyclohexanone 1 while Nyiko proposed Method B that started from hydroxymethylcyclohexane 3. Each student believed that their proposed method is better than the other. (Scheme below) (1) 1 Ph THF A Ph Ph B H₂SO4 100 °C 3 OH What is the name of the reaction that is followed by reaction Method A?
Propose a method to separate a mixture containing phenol, benzoic acid, naphthalene, and p-nitroaniline. Phenol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. Benzoic acid is soluble in either sodium hydroxide or sodium bicarbonate solutions. Write out the structures of the molecules in your scheme.
Starting with benzene, toluene, or phenol as the only sources of aromatic rings, show how to synthesize the following. Assume in all syntheses that mixtures of ortho-para products can be separated into the desired isomer. Q.)p-Chlorobenzoic acid
When CO2 is bubbled through a solution of benzyl magnesium bromide, and the mixture is then acidified, the product is phenylacetic acid. Any unreacted benzyl magnesium bromide is converted to toluene in the acidification step. 1. Write the complete reaction sequence for the process, showing product and byproduct. 2. How could you separate phenylacetic acid from toluene?