In complexometric titration ‘the reaction with analyte should be rapid and complete’ give reason with suitable justification for the above statement.
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In complexometric titration ‘the reaction with analyte should be rapid and
complete’ give reason with suitable justification for the above statement.
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- Water sample from different river water was subjected to a qualitative alkaline analysis by titrating against 0.1250 MHC1 and using phenolphthalein and bromocresol green end point. The table below shows the volumes of acid needed to titrate 25.00-mL portions of each sample and their corresponding end point, separately. Use this information to deduce the composition of the solutions. Calculate the molar concentration of each solute. Volume (mL) Phenolphthalein end Bromocresol green Solute identity concentration end point Volume (mL) Molar Sample point 22.40 of solute/s 1 22.41 2 0.00 33.40 3 15.67 42.13 4 29.64 36.42A 10.00cm3 portion of the 100.00cm3 HCl solut was taken from the volumetric flask and was titrated with KOH (aq). It was neeutralized by 24.35cm3 of potassium hydroxide od concentration 0.0500moldm-3. Calculate the concentrat of the original concentrated hydrochloric acid in moldm-3.A sample containing BaCl, 2H,0, KCI and inert material weighed 0.8417 g. After heating the sample at 160°C for 45 min, it weighed 0.8076 g. The sample was then dissolved in water and treated with a slight excess of AgNo,. The resulting precipitate was collected and found to weigh 0.5847 g. Calculate the % Bacl,-2H,0 and % KCI in the sample. 3.
- (3). Write short notes on displacement titration with suitable example.1. A 0.3516 g sample of commercial phosphate detergent was ignited at a heat to destroy the organic matter. The residue was taken up in hot HCI which converted P to H3PO4. The phosphate was precipitated as MGNH4PO4.6H2O by addition of Mg+ followed by aqueous NH3. After being filtered and washed, the precipitate was converted to Mg2P2O7 by ignition at 1000 OC. This residue weighed 0.2161 g. Calculate the percent P (30.974) in the sample? Ans 17.11%Determination of sodium carbonate by acidimetric titration involves: Direct titration by acid solution with usage as indicator either methyl orange or phenolphthalein; heating of analyte till 70° C; Direct titration by acid solution with sequential usage of 2 indicators: methyl orange and phenolphthalein; Back titration by acid solution with usage as indicator phenolphthalein;
- What wt of magnetite should be taken for analysis in order that after converting to a precipitate of Fe2O3.xH2O, the percentage of Fe3O4 in the sample can be found by multiplying the wt in grams of the ignited precipitate (Fe2O3) by 100.A suitable target for the titration is 30.0 cm3 of 0.025 moldm-3 Br2(aq) Justify why a much smaller target titre would not be appropriate Calculate the amount in moles of bromine in the target titer Justification? calculate a suitable massof alive oil to transfer to the volumetric flask using your answer to of above question and the structure of Y Assume that the olive oil contains 85/- of Y by mass (If you were unable to calculate the amount of bromine in the target titer,you should assume it is 6.25×10^-8 mol .this in not the correct amount)The arsenic in a 1.010 g sample of a pesticide was converted to H3AsO4 by suitable treatment. The acid was then neutralized, and exactly 40.00 mL of 0.06222M AgNO3 was added to precipitate the arsenic quantitatively as Ag3AsO4. The excess Ag in the filtrate and in the washings from theprecipitate was titrated with 10.76 mL of 0.1000MKSCN; the reaction wasAg+ + SCN-→ AgSCN(s) Calculate the percent AsO3 in the sample.
- The concentration of ammonia in a cleaning product was determined by back titration.Firstly, 10.00 cm3 of the cleaning product was pipetted into a large conical flask,containing 250.00cm3 of 0.50 mol/l HCl to give Solution A.Following a period of reaction and shaking, 50.00cm3 of Solution A was removed anddiluted to 250 cm3 with water in a volumetric flask to give Solution B.20 cm3 samples of Solution B were titrated against 0.05 mol/l Na2CO3 solution, givingan average titre of 12.45 cm3. i) Write equations for the reactions that have taken place.ii) Determine the concentration of NH3 in the original cleaning product in mol/l,g/l, ppm, and % w/v.A series of solutions containing NaOH, Na.CO, and NaHCO, alone or in compatible combination, was titrated with o.1202 needed to titrate 25.00-mL portions of each solution to (1) a phenolphthalein and (2) a bromocresol green end point. Use this information to deduce the composition of the solutions. In addition, calculate the mass in milligrams of each solute per milliliter of solution. M HCI. Tabulated below are the volumes of acid (2) (1) (а) 22.42 (Ъ) 15.67 (c) 29.64 (d) 16.12 (е) о.00 22.44 42.13 36.42 32.23 33.333Five drops of dichlorofluorescein have been added to a solution containing 0.800 g sample which required 25.30 mL of 0.100 M AgNO3. (a) Identify the type of argentometric titration method used.
