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Melting Point Lab

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Experiment #1: Purification of a Solid: Crystallization and Melting Point: Joseph Katz and Melissa Colwell Binghamton University, Department of Chemistry, Binghamton, New York 13902 Introduction: One of the most important parts of this experiment was the concept of the melting point. The melting point is the temperature at which a substance turns from a solid into a liquid. Every substance has a specific temperature of melting point although any impurities in a substance will lower the temperature required to melt it. This means that as more impurities are removed, the closer the melting point of a substance will get closer to the real melting point. …show more content…

The material that was selected had a yellow coloring which followed through to the solution created when the sample was dissolved into the distilled water. The charcoal that was added took a large amount of the color out of the solution. As a result, it was decided to only use one aliquot of charcoal. The charcoal only filtered out the impurity and not the sample itself due to differences in boiling point. The charcoal (with the impurities) was removed through a hot gravity filtration after being heated. The solution that was left over had a faint yellow color to it. This solution was then cooled in an ice-bath for about thirty minutes in order to start the crystallization process. The crystals were dried through vacuum filtration and put into a vial which was then weighed, showing that 91.67% of the initial substance was …show more content…

Although the amount recovered was high, the crystals still had a yellow color, showing that impurities remained in the sample. However, the melting point was within the range of the acid identified. Conclusion: The experiment determined that the unknown sample was phthalic acid due to the melting point of 208.9 degrees Celsius. The correction of the machine was found to be 0.3 degrees Celsius, and it was machine #5. The percent recovered was determined to be 91.67%. Acknowledgements: I would like to acknowledge my lab partner Melissa Colwell for assistance during the lab. References: 1) Organic Chemistry Laboratory Manual, Spring 2015 Edition, Department of Chemistry, Binghamton University, Binghamton New York, 2012 pp 3-4, 77-86. 2) "Liquids." Melting Point, Freezing Point, Boiling Point. http://chemed.chem.purdue.edu/genchem/topicreview/bp/ch14/melting.php. 3) Lide, David R. CRC Handbook of Chemistry and Physics: A Ready-reference Book of Chemical and Physical Data. Boca Raton, FL: CRC, 1994.

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